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Nano-sclerometry measurements of superhard materials and diamond hardness using scanning force microscope with the ultrahard fullerite C60 tip

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Abstract

The new procedure for the hardness measurements of superhard materials including diamond using the scanning force microscope with the ultrahard fullerite C60 tip was developed. It is shown that diamond is plastically deformed under the indentation by the ultrahard fullerite indenter at room temperature. Now the correct measurements of diamond hardness have become possible. The hardness values measured are 137 ± 6 and 167 ± 5 GPa for the diamond faces (100) and (111), respectively.

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References

  1. M.J. Mayo, R.W. Siegel, A. Narayanasamy, and W.D. Nix, J. Mater. Res. 5, 1073 (1990).

    Article  CAS  Google Scholar 

  2. J. B. Pethica, R. Hutchings, and W. C. Oliver, Philos. Mag. A 48, 593 (1983).

    Article  CAS  Google Scholar 

  3. Q. Ma and D. R. Clarke, J. Mater. Res. 10, 853 (1995).

    Article  CAS  Google Scholar 

  4. M. F. Doerner and W. D. Nix, J. Mater. Res. 1, 601 (1986).

    Article  Google Scholar 

  5. D. Scholl, M. P. Everson, and R. C. Jaklevic, J. Mater. Res. 10, 2503 (1995).

    Article  Google Scholar 

  6. E. T. Lilleodden, W. Bonin, J. Nelson, J.T. Wyrobek, and W. W. Gerberich, J. Mater. Res. 10, 2162 (1995).

    Article  CAS  Google Scholar 

  7. B. Bhushan and V. N. Koinkar, Appl. Phys. Lett. 64, 1653 (1994).

    Article  CAS  Google Scholar 

  8. J. Wilks and E. Wilks, Properties and Applications of Diamond (Butterworth–Heinemann Ltd., Oxford, 1991).

    Google Scholar 

  9. V. Blank, S. Buga, N. Serebryanaya, V. Denisov, G. Dubitsky, A. Ivlev, B. Mavrin, and M. Popov, Phys. Lett. A 205, 208 (1995).

    Article  CAS  Google Scholar 

  10. V. Blank, S. Buga, N. Serebryanaya, G. Dubitsky, S. Sulyanov, M. Popov, V. Denisov, A. Ivlev, and B. Mavrin, Phys. Lett. A 220, 149 (1996).

    Article  CAS  Google Scholar 

  11. R. S. Ruoff and A. L. Ruoff, Nature 350, 663 (1991).

    Article  Google Scholar 

  12. R. Howland and L. Benatar, A Practical Guide to Scanning Probe Microscopy (Park Scientific Instruments, Mountain View, CA, 1993).

    Google Scholar 

  13. N. A. Burnham, R. J. Colton, and H. M. Pollock, Nanotechnology 4, 64 (1993).

    Article  CAS  Google Scholar 

  14. J. Tansock and C. C. Williams, Ultramicroscopy 42–44, 1464 (1992).

    Article  Google Scholar 

  15. K. V. Gogolinsky, V. N. Reshetov, and P. I. Markov, Proc. Int. Conf. Computer Methods and Inverse Problems in Non-Destructive Testing and Diagnostics (Minsk, Belarus, 1995), pp. 267–270.

    Google Scholar 

  16. V. Lyssenko, A. Astashenkov, K. Gogolinsky, and V. Reshetov, Proc. 7th Int. Conf. Metrology and Properties of Engineering Surfaces (Göteborg, Sweden, 1997) (in press).

  17. J. Mencik and M. V. Swain, J. Mater. Res. 10, 1491 (1995).

    Article  CAS  Google Scholar 

  18. V. K. Grigorovich, Hardness and Microhardness of Metals (Nauka, Moscow, 1976, in Russian).

    Google Scholar 

  19. N. V. Nonikov, S. N. Dub, and V. I. Mal’nev, Superhard Materials (in Russian), 1992, No. 5, p. 5.

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Blank, V., Popov, M., Lvova, N. et al. Nano-sclerometry measurements of superhard materials and diamond hardness using scanning force microscope with the ultrahard fullerite C60 tip. Journal of Materials Research 12, 3109–3114 (1997). https://doi.org/10.1557/JMR.1997.0406

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  • DOI: https://doi.org/10.1557/JMR.1997.0406