Abstract
The new procedure for the hardness measurements of superhard materials including diamond using the scanning force microscope with the ultrahard fullerite C60 tip was developed. It is shown that diamond is plastically deformed under the indentation by the ultrahard fullerite indenter at room temperature. Now the correct measurements of diamond hardness have become possible. The hardness values measured are 137 ± 6 and 167 ± 5 GPa for the diamond faces (100) and (111), respectively.
Similar content being viewed by others
References
M.J. Mayo, R.W. Siegel, A. Narayanasamy, and W.D. Nix, J. Mater. Res. 5, 1073 (1990).
J. B. Pethica, R. Hutchings, and W. C. Oliver, Philos. Mag. A 48, 593 (1983).
Q. Ma and D. R. Clarke, J. Mater. Res. 10, 853 (1995).
M. F. Doerner and W. D. Nix, J. Mater. Res. 1, 601 (1986).
D. Scholl, M. P. Everson, and R. C. Jaklevic, J. Mater. Res. 10, 2503 (1995).
E. T. Lilleodden, W. Bonin, J. Nelson, J.T. Wyrobek, and W. W. Gerberich, J. Mater. Res. 10, 2162 (1995).
B. Bhushan and V. N. Koinkar, Appl. Phys. Lett. 64, 1653 (1994).
J. Wilks and E. Wilks, Properties and Applications of Diamond (Butterworth–Heinemann Ltd., Oxford, 1991).
V. Blank, S. Buga, N. Serebryanaya, V. Denisov, G. Dubitsky, A. Ivlev, B. Mavrin, and M. Popov, Phys. Lett. A 205, 208 (1995).
V. Blank, S. Buga, N. Serebryanaya, G. Dubitsky, S. Sulyanov, M. Popov, V. Denisov, A. Ivlev, and B. Mavrin, Phys. Lett. A 220, 149 (1996).
R. S. Ruoff and A. L. Ruoff, Nature 350, 663 (1991).
R. Howland and L. Benatar, A Practical Guide to Scanning Probe Microscopy (Park Scientific Instruments, Mountain View, CA, 1993).
N. A. Burnham, R. J. Colton, and H. M. Pollock, Nanotechnology 4, 64 (1993).
J. Tansock and C. C. Williams, Ultramicroscopy 42–44, 1464 (1992).
K. V. Gogolinsky, V. N. Reshetov, and P. I. Markov, Proc. Int. Conf. Computer Methods and Inverse Problems in Non-Destructive Testing and Diagnostics (Minsk, Belarus, 1995), pp. 267–270.
V. Lyssenko, A. Astashenkov, K. Gogolinsky, and V. Reshetov, Proc. 7th Int. Conf. Metrology and Properties of Engineering Surfaces (Göteborg, Sweden, 1997) (in press).
J. Mencik and M. V. Swain, J. Mater. Res. 10, 1491 (1995).
V. K. Grigorovich, Hardness and Microhardness of Metals (Nauka, Moscow, 1976, in Russian).
N. V. Nonikov, S. N. Dub, and V. I. Mal’nev, Superhard Materials (in Russian), 1992, No. 5, p. 5.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Blank, V., Popov, M., Lvova, N. et al. Nano-sclerometry measurements of superhard materials and diamond hardness using scanning force microscope with the ultrahard fullerite C60 tip. Journal of Materials Research 12, 3109–3114 (1997). https://doi.org/10.1557/JMR.1997.0406
Received:
Accepted:
Published:
Issue date:
DOI: https://doi.org/10.1557/JMR.1997.0406


